puncture hole in the canâs lid, drawing a sample of air, and turned to the large instrument set on the steel table. Its Plexiglas panel revealed an extended capillary tube. As she injected the syringeâs invisible contents into the machineâs capillary tube, I heard a starting gun go off in my head.
The great race of Gas Chromatography Mass Spectrometer.
âThis is my fourth run on these volatiles,â she said. âJust so you know I didnât pull these results out of thin air, so to speak.â
âFour runs?â
âI thought something was wrong.â
Inside the instrument a small furnace heated the vapor within the capillary tube, exciting the compounds and breaking their bonds. As they separated into individual molecules, the smaller elements sprinted through the capillary tube, while the larger molecules lumbered for the finish line. Nettie pushed the safety goggles up on her forehead and keyed up the computer monitor.
Within moments colored bar graphs started rising and falling on the monitor, showing individual weights and speed of travel for each molecule. Call me a nerd; I loved how GCMS was like a track race with no names on the runners. Like being told thereâs a 119-pound female who does the hundred-yard dash in thirteen seconds. Your job was to figure out her name.
Back in the early days, we matched molecules by combing through chemistry textbooks. These days computers did all the work.
âThatâs what Iâm talking about,â Nettie said as the mass spec painted its final graph, tossing names on the monitor. âThe accelerant used to light that cross was mustard gas. And something called lewisite.â
âMustard gas?â I leaned forward, staring at the results. âFrom what, World War I?â
But she was already walking back to her desk down the hall from the instrument room. The smallest forensics department in the lab, mineralogy was tucked into the buildingâs north side. Nettie dropped into a swivel chair, stubbing her Birkenstock into the floor to pivot and reach under her desk, pulling out a folder.
âMustard gas isnât even the most peculiar compound,â she said. âWait until you meet lewisite.â
âMineral?â
âDeadly chemical compound,â she said cheerfully. âAll by itself, lewisite is nasty stuff. But add in some mustard gas and the toxicity goes off the charts. Whoever used these chemicals wanted to make sure that cross burned.â
She flipped the folder open so I could see.
The clinical photographs magnified five and ten times showed angry rashes that oozed blood and pus.
But Nettie seemed unfazed.
âIn addition to the skin trauma,â she said, âlewisite produces convulsions, vomiting, and catatonic states. Sort of like what happens to me when somebody hands me a Barbie doll. Mustard gas does about the same. Burns, blinds people. But it smells like geraniums.â
âWhat?â
âYeah, thatâs what I read. Who knew? I take that back. Whoever put this stuff on the grass knew. Or theyâre dead from contact.â She tossed me the folder. âYour copy, all the data.â
Opening the file, I glanced over her notes. Her penmanship surprised me. Scrolled and flourishing, as feminine as a wedding invitation, somehow it made the medical photos even more gruesome. âI appreciate the quick turnaround. Thank you.â
âBut youâre going to tell me somethingâs wrong.â
âThis happened in rural Virginia. See what Iâm saying?â
She noddedâa quick, excited gestureâand combined with the spray of freckles across her nose and the faded jeans, she looked all of fifteen. âI wondered about that too. So I went through the labâs back files on cross burnings. To check accelerants.â
âAnd?â
âNothingâs even close.â
âNothing?â
âThey mostly use gasoline and